石墨烯具有眾多優異特性，於近幾年蓬勃發展，無論是針對其理論特性亦或是實驗量測皆掀起一陣熱潮，其優異特性如超高電子遷移率、電導率、熱導率、透光性及機械特性等，將被廣泛應用於各學界，亦因石墨烯擁有眾多特性，促使本實驗對其進行探究。
石墨烯製備方法許多，除最先利用膠帶之機械剝離法，發現了單層石墨烯外，另有其他眾多方式，如：氧化還原法、化學氣相沉積法、碳化矽延展生長法等，以及於2010年發表至Nature期刊初次利用固態碳源製備石墨烯之方法，本實驗石墨烯製備方法即採用固態碳源製備石墨烯。
本實驗利用高分子聚合物PMMA塗佈於完成預處理之25 m厚的銅箔上並進行烘烤後，將處理完成之樣品置於紅外線黃金鍍膜快速升溫加熱爐（RTA）中，執行石墨烯高溫製程，藉由調控製程溫度、塗佈轉速、氣體流量、降溫條件等製備環境之操控以製備石墨烯。
使用銅箔與PMMA作為基板與碳源，除了銅箔取得容易，其還具有催化碳分子堆積於銅箔表面之特性，而固態碳源PMMA亦是實驗材料中容易取得之材料，利用PMMA成功製備出石墨烯，可藉以推廣應用至各項含碳物質，生活環境中眾多物質皆有機物，可取之運用做為製備石墨烯之碳源。
本實驗製備石墨烯之過程，藉由縝密之實驗條件改善後，本實驗結果成功製備石墨烯成膜於銅箔表面，將樣品進行轉移至載玻片，利用拉曼光譜儀檢測樣品品質與層數，可成功生成單層與雙層石墨烯，表面型態則藉由光學顯微鏡進行檢測。

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