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研究生: 游宇豐
Yu, Yu-Fong
論文名稱: 吸附氣體在鈮(100)切面上功函數與場發射電流穩定性的量測
Measurement of workfunction and instability of field emission current of adsorbing inert gas on Nb(100)
指導教授: 傅祖怡
Fu, Tsu-Yi
黃英碩
Hwang, Ing-Shouh
學位類別: 碩士
Master
系所名稱: 物理學系
Department of Physics
論文出版年: 2015
畢業學年度: 103
語文別: 中文
論文頁數: 81
中文關鍵詞: 場發射鋪覆氣體鈮針
英文關鍵詞: field emission, adsorption gases, niobium
論文種類: 學術論文
相關次數: 點閱:169下載:3
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  • 我們利用電化學蝕刻方法蝕刻純鈮針,製作出針徑接近50nm以內的針尖後置入超高真空中,經過反覆加熱退火處理得到一熱穩態結構,此結構為四個{310}皺化擠壓{100}切面。
    我們利用惰性氣體(Xe、Ne)給予腔體不同的鋪覆環境,再量測由純鈮{100}切面發射出來的電流與施加的偏壓去繪出FN圖,再由FN圖上斜直線斜率經計算後得到鈮{100}的表面功函數。
    發現鋪覆此兩種氣體後,鈮{100}切面的表面功函數會下降,下降幅度會隨著鋪覆的環境而變化,兩種氣體有所謂的最佳鋪覆環境,而在最佳鋪覆環境下的鈮{100}表面功函數會有最大的下降幅度,經過三次實驗的統計結果顯示在最佳鋪覆環境下,鈮{100}面鋪覆Xe後的表面功函數下降幅度比鋪覆Ne明顯。
    並且我們量測純鈮{100}切面在最佳鋪覆環境下場發射電流三十分鐘後的穩定性,我們調控場偏壓、平均電流並觀察穩定性上的變化,發現純鈮{100}面的發射電流穩定性沒有比鋪覆Xe在最佳鋪覆環境下的電流穩定。

    We fabricate a thermally stable pure niobium tip with a small (100) facet faceting structure surrounded by four {310} surfaces by thermal treatment in UHV.
    We observe the thermally stable structure by field ion microscopy (FIM) and measure field emission current from the niobium (100) facet with a Faraday cup. After exposing the tips under various gas (Ne, Xe) environments(1 Langmuir), we measure the emission currents at various applied voltages. Variation of field-emission work functions due to different absorption gases can be observed from the illustrated F-N plots. We find Xe gas noticeably reduces the work function of the niobium (100) facet.
    We measure stability of the field emission current from niobium {100} facet with Faraday cup in 30 minunits.

    致謝.............................................................I 摘要............................................................II Abstract.......................................................III 目錄............................................................IV 第一章 緒論.......................................................1 1-1.研究動機.....................................................1 第二章 實驗原理...................................................5 2-1.場發射顯微鏡的理..............................................5 2-2.場離子顯微鏡的成像原理........................................12 2-3.場離子化制...................................................15 2-4.場退吸附與場發...............................................18 2-5.表面皺化機制.................................................21 2-6.場離子影像說明...............................................23 3-1.場離子顯微鏡的儀器裝置........................................26 3-2.樣品製備....................................................34 第四章 實驗結果與分析.............................................40 4-1.成長鈮(100).................................................40 4-2.鈮在同樣氣體在不同鋪覆環境下,(100)切面的場發射特性量測.........50 4-3.鋪覆氣體後鈮(100)切面的場發射電流穩定性........................64 第五章 結論......................................................75 5-1.製備鈮針方法.................................................75 5-2.成長鈮(100)切面..............................................75 5-3.鋪覆氣體的鈮(100)切面場發射功函數.............................76 5-4.鋪覆氣體的鈮(100)切面發射電流穩定性...........................76 附錄............................................................78 參考文獻........................................................80

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