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研究生: 李柏璋
Li, Po-Chang
論文名稱: 以氙氣作為單原子針離子發射源之研究
The investigation of xenon in gas field ion source
指導教授: 傅祖怡
Fu, Tsu-Yi
黃英碩
Hwang, Ing-Shouh
學位類別: 碩士
Master
系所名稱: 物理學系
Department of Physics
論文出版年: 2015
畢業學年度: 103
語文別: 中文
論文頁數: 54
中文關鍵詞: 單原子針場離子顯微鏡
英文關鍵詞: Single atom tip, Field ion microscope
論文種類: 學術論文
相關次數: 點閱:106下載:1
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  • 本實驗利用場離子顯微鏡(Field Ion Microscope, FIM),並使用本實驗室製作的附銥鎢單原子針作為場發射源,探討以氙氣作為氣體離子源的離子電流特性,並與氦氣離子源互相比較。
    我們透過液態氮降溫針尖,並量測在不同溫度下,氙氣離子的飽和電流值,發現溫度降低接近至150 K附近時,離子電流有急遽增加 的趨勢,推測最佳工作溫度應為150 K以下附近。之後量測氙氣離子束的電流穩定性,與氦氣離子束的電流穩定性相當。透過以氙氣作為成像氣體的單原子針影像,計算出其離子束的張角小於1度,是非常集中的離子源,且角強度及亮度也有很好的表現。
    氙氣離子束在150 K的工作溫度下,與氦氣離子束在22 K的工作溫度下的能力相近。若希望將氣體場發射離子源(Gas Field Ion Source, GFIS)應用在二次質譜儀(Secondary Ion Mass Spectroscopy, SIMS),則氙氣就具有成為此種離子源的潛力。

    Xenon gas is the ion source of gas field ion source (GFIS), which emitter is the Ir/W <111>single atom tip in this research. We found the properties of xenon ion beam, and compared with helium ion beam.
    We used liquid nitrogen to cool the tip, and measured the saturation ion current of xenon in different tip’s temperature. We found that when the temperature was approaching 150K, the ion current was increasing quickly. We guessed the optimum temperature for xenon ion beam is below 150K. Then we measured the stability of xenon ion beam. It’s as good as helium ion beam. Finally we calculated the open angle of xenon ion beam, which was in 1 degree, by its image in the field ion microscopy. It’s also has a good angular intensity and brightness.
    Xenon ion beam has the same ability in 150K with helium ion beam in 22K. If we want to apply the GFIS in secondary ion mass spectroscopy (SIMS), xenon is the good choice for it.

    英文摘要 中文摘要 第一章 緒論 1-1 研究動機………………………………………………………1 1-2 單原子針………………………………………………………5 第二章 實驗原理 2-1 場發射顯微鏡……………………………………………11 2-2 場離子顯微鏡……………………………………………12 2-3 場蒸發與場退吸附…………………………………18 2-4 場離子影像…………………………………………………22 2-5 皺化機制………………………………………………………27 2-6 氣體供應函數與離子電流……………………27 第三章 實驗儀器架設與實驗方法 3-1 場離子顯微鏡的組成………………………………29 3-2 單原子針的製備…………………………………………35 第四章 實驗結果與分析 4-1 Xe離子飽和電流及電流穩定性……………39 4-2 Xe最佳工作溫度…………………………………………44 4-3 Xe離子束角強度計算………………………………48 第五章 結論………………………………………………………………52 參考文獻 ……………………………………………………………………………53

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