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Author: 蘇政湟
Thesis Title: 振動樣品磁量儀及樣品檢測
Production of Vibarting Sample Magnetometer and measurment of sample
Advisor: 謝振傑
Chieh, Jen-Jie
洪姮娥
Horng, Herng-Er
Degree: 碩士
Master
Department: 光電工程研究所
Graduate Institute of Electro-Optical Engineering
Thesis Publication Year: 2014
Academic Year: 102
Language: 中文
Number of pages: 39
Keywords (in Chinese): VSM振動樣品磁量儀樣品檢測
Thesis Type: Academic thesis/ dissertation
Reference times: Clicks: 411Downloads: 4
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  • 本系統是以直流磁場及振動馬達驅動的振動樣品磁力儀(Vibarting SampleMagnetometer),系統的振幅為4 mm (上下 2 mm),可控制頻率範圍為 30 Hz。樣品管材質使用塑鋼製成,為了不使樣品管被磁化干擾到訊號量測結果。樣品棒則以25.5 公分長之纖維強化高分子複合材料(FRP)製成,因材料質輕又強固。樣品管則直接接到樣品棒的底端。系統使用上更人性化,使用者可視樣品種類來決定使用何種樣品棒以及磁場走向來進行量測。因此,將系統振動器、感應線圈組與電磁鐵三者設計成獨立裝置,使用上可視需求簡易設定磁走向或感應線圈組合。系統標準是以實驗室現有之振動樣品磁力儀(Vibarting Sample Magnetometer)測量鎳片的數據作為比較依據,兩者數據比較證明我們建構之磁力計具有一定之準確度。對磁流體的量測可達0.4 µemu . 最後我們將自製的機台用來量測肝癌AFP免疫檢測實驗。

    摘要............................................................................................................ ….ii 目錄............................................................................................................ ….iii 第一章 緒論 ............................................................................................... ….1 1.1 振動樣品磁力儀(VSM) ............................................................ ….2 1.2肝癌AFP免疫檢測........................................................................ ….3 第二章 實驗原理 ....................................................................................... ….4 2.1 VSM ........................................................................................... ….4 2.2 磁學原理 .................................................................................. ….9 2.2.1 順磁性與反磁性 ................................................................. ….11 2.2.2 鐵磁性、反鐵磁性與亞鐵磁性 ......................................... ….13 2.3 磁流體 .................................................................................... ….15 2.3.1 磁流體簡述 ......................................................................... ….15 2.3.2 磁流體的應用 ..................................................................... ….17 第三章 自製系統架構 ............................................................................. ….18 第四章 應用於肝癌AFP免疫檢測 ........................................................... ….25 第五章 實驗結果與討論 ......................................................................... ….28 第六章 結論與未來展望 ......................................................................... ….33 6.1 結論 ........................................................................................... ….33 6.2 未來展望 ................................................................................... ….33 參考文獻 .................................................................................................... ….34

    1. http://en.wikipedia.org/wiki/Magnetism
    2. S. Foner, digital Encyclopedia of Applied Physics, “MEASUREMENT OF
    MAGNETIC PROPERTIES AND QUANTITIES”, WILEY-VCH Verlag GmbH
    & Co KGaA,
    3. S. Foner, “Versatile and Sensitive Vibrating-Sample Magnetometer”, Rev. Sci.
    lnstrum. vol. 30, no. 7, 1959, pp. 548-557.
    4. S. Foner, “Further improvements in vibrating sample magnetometer sentivity”,
    Rev. Sci. lnstrum., vol. 46, no. 10, October 1975. pp. 1425-1426.
    5. E. O. Samwel, T. Bolhuis and J. C. Lodder, “An alternative approach to vector
    vibrating sample magnetometer detection coil setup”, Rev. Sci. Instrum. vol.69, no.
    9, 1998. pp. 3204-3209.
    6. J.P.C. Bernards, “Design of a detection coil system for a biaxial vibrating sample
    magnetometer and some applications”, Rev. Sci. Instrum. vol. 64, no.7, 1993 ,
    pp. 1918-1930.
    7. C. Johansson and M. Hanson, “Influence of Sample Geometry in a Vibrating
    Sample Magnetometer”, IEEE Transactions of Magnetics. vol. 30, no. 2, 1994, pp.
    1064-1066.
    8. K. H. Shin, K. I. Park, Y. Kim, and G. Sa-Gong, “Vibrating sample magnetometer
    using a multilayer piezoelectric actuator”, phys. stat. sol. (b), vol. 241, no. 7, 2004,
    pp. 1633–1636.
    9. V I Nizhankovskii and L B Lugansky, “Vibrating sample magnetometer with a
    step motor”, Meas. Sci. Technol. vol. 18 , 2007, pp. 1533–1537.
    10. S. Foner, “ The vibrating sample magnetometer: Experiences of a volunteer
    (invited)”, J. Appl. Phys., vol. 79, no.8, 1996, pp. 4740-4745.
    11. A. Zieba and S. Foner, “ Detection coil, sensitivity function, and sample geometry
    effects for vibrating sample magnetometer”, Rev. Sci. Instrum. vol. 53, no. 9, 1982,
    71
    pp. 1344.
    12. 徐光宏,磁性流變流體之製程研究,碩士論文,國立成功大學機械工程系,
    台南,2002。.
    13. K. Enpuku, D. Kuroda, A. Ohba, T.Q. Yang, K. Yoshinaga, T. Nakahara, H. Kuma
    and N. Hamasaki, “Biological Immunoassay Utilizing Magnetic Marker and High
    Tc Superconducting Quantum Interference Device Magnetometer”, Jpn. J. Appl.
    Phys. vol. 42, 2003, pp. L1436-L1438.
    14. K. Enpuku, K. Inoue, K. Soejima, K. Yoshinaga, H. Kuma, and N. Hamasaki,
    “Magnetic Immunoassays Utilizing Magnetic Markers and a High-Tc SQUID”,
    IEEE Transactions on Applied Superconductivity. vol., 15, no. 2, 2005, pp. 660.
    15. 楊謝樂,「磁性奈米粒子於生物醫學上之應用」,物理雙月刊,第二十八卷,
    第四期,2006,第692-697頁。
    16 楊鴻昌,「SQUID生物磁學:醫學應用與展望」,物理雙月刊,第二十九卷,第
    四期,2007,第799-814頁。
    17. R. Held, “Improving A Vibrating Sample Magnetometer” Stetson University,
    Senior Research Project, unpublished, 1993, pp. 1.
    18. Abbess Technical Notes: Magnetic Measuring Techniques, July 6, 2000. P1-P5.
    19. Mike Jackson, “This thing called Flux (a primer)”, The IRM Quarterly, vol. 18,
    no. 1, 2008, pp. 10.
    20. A. Niazi, P. Poddar and A. K. Rastogi, " A precision, low-cost vibrating sample
    magnetometer”, Current Science, vol. 79, no. 1, 2000, pp.99-100.
    21. V. I.Maksimochkin, V. I. Trukhin, N. M. Garifullin, and N. A. Khasanov, “An
    Automated High-Sensitivity Vibrating-Coil Magnetometer”, Instruments and
    Experimental Techniques, vol. 46, no.5, 2003, pp.132-137.
    22. J.P. Anderson and R. J. Bloter, “Permeability and Hysteresis Measurement”, Copy
    right 2000 CRC Press LLC. pp. 2-4.
    23. 張煦、李學養譯,磁性物理學,台北: 聯經出版社,1982,第9-11頁。
    24. G.A. van Ewijk, Phase behavior of mixtures of magnetic colloids and
    non-adsorbing polymer, Ph. D. Thesis, Utrecht University, Utrecht, Netherlands.
    72
    2001.
    25. S. Odenback, “Recent progress in magnetic fluid research”, J. Phys.: Condens.
    Matter, vol. 16, 2004, R1135-R1150.
    26. E. E. Bibik, B. Y. Matgullin, Y. L. Raikher and M. I. Shliomis, “The magnetostatic
    properties of colloidal magnetite”, Magnetohydrodynamics, vol.9, no.1, 1973, p.p
    58-62.
    27. 謝振傑 超導量子干涉儀系統用於磁性奈米粒子的磁性生醫領域 4/16 2012
    28. http://www.ferrolabs.com/en/information/33/
    29. Hong CY, Wu CC, Chiu YC, Yang SY, Horng HE, Yang HC: Magnetic
    susceptibility reduction method for magnetically labeled immunoassay. Appl Phys
    Lett , vol. 88, 2006, pp. 212512-1-212512-3.
    30. Hong CY, Chen WH, Jian ZF, Yang SY, Horng HE, Yang LC, Yang HC:
    Wash-free immunomagnetic detection for serum through magnetic susceptibility
    reduction. Appl Phys Lett, vol. 90, 2007, pp. 74105-1-74105-3.
    31. 楊謝樂,「高靈敏度磁減量生醫檢測原理及應用」,台灣磁性技術協會會訊,
    第51期,2010,第35-38頁。
    32. Yang SY, Jian ZF, Chieh JJ, Horng HE, Yang HC, Hong CY: Wash-free,
    antibody-assisted magnetoreduction assays on orchid viruses. J Virol Methods,
    vol. 149, 2008, pp. 334-336.
    33. http://olddoc.tmu.edu.tw/chiaungo/h-check/h-chk-CRP.htm, (Posted on May 10,
    1996; Updated Apr. 30 , 2005) 吳昭新醫師著,C-反應蛋白。
    34. Stanford Research Systems, Operating Manual: "Model SR530 lock-in amplifier",pp.28-29.

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